Methyl (R)-(1-hydroxy-3-methylbutan-2-YL)carbamate → (4R)-4-(Propan-2-yl)-1,3-oxazolidin-2-one

https://huagongshe.com/de/reaction/2371699

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Methyl (R)-(1-hydroxy-3-methylbutan-2-YL)carbamate	HCID 15714133	—
Lösungsmittel	Toluene	HCID 1140	—
Produkt	(4R)-4-(Propan-2-yl)-1,3-oxazolidin-2-one	HCID 641505	—

Reaktionsbedingungen

Temperatur	150 °C

Reaktionsschritte

27.2 g (168.7 mmol) of the compound from Example V are dissolved in 400 ml of toluene and stirred under reflux in an oil bath at 150° C. while passing in nitrogen.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US05095006
Quelldatensatz	uspto-grants-1992_03
ORD ID	ord-7518c1e32d2b4d4fadb76a3e57559c1e
Quellennotiz	uspto-grants-1992_03