HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethylformamide → 4-Chloro-7-nitroquinazoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethylformamide | HCID 6228 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 7-Nitroquinazolin-4(3H)-one | HCID 86222800 | — |
| Produkt | 4-Chloro-7-nitroquinazoline | HCID 830680 | — |
Reaktionsschritte
To a solution of 7-nitroquinazolin-4(3H)-one (2.0 g, 10.5 mmol) in 40 ml thionyl chloride was added 0.8 ml of DMF and the mixture was heated at reflux overnight then evaporated to dryness to provide crude 4-chloro-7-nitroquinazoline.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08642582B2 |
| Quelldatensatz | uspto-grants-2014_02 |
| ORD ID | ord-f0f7d6401cd4487e98e4fe40bbd46dba |
| Quellennotiz | uspto-grants-2014_02 |