HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(4-Iodophenyl)ethan-1-one → 1-[4-(3,3-Dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepin-7-ylethynyl)-phenyl]-ethanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(4-Iodophenyl)ethan-1-one | HCID 72869 | — |
| Edukt | 7-Ethynyl-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine | HCID 59852695 | — |
| Produkt | 1-[4-(3,3-Dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepin-7-ylethynyl)-phenyl]-ethanone | HCID 59852693 | — |
Reaktionsschritte
The title compound is prepared in analogy to example 1 from 7-ethynyl-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine (6) (example 1d) and 1-(4-iodo-phenyl)-ethanone. MS (ESI) 320.2 (M•)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07459480B2 |
| Quelldatensatz | uspto-grants-2008_12 |
| ORD ID | ord-fbe8ec5045bd41b1b9a90e85259d1044 |
| Quellennotiz | uspto-grants-2008_12 |