5-Chlorovaleryl chloride → 9-(5-chloropentanoyl)-1,2,6,7-tetrahydropyrido[3,2,1-ij]quinolin-3(5H)-one

HRID 2374569Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2374569
[CH2:1]1[C:10]2[C:5]3=[C:6]([CH2:11][CH2:12][C:13](=[O:14])[N:4]3[CH2:3][CH2:2]1)[CH:7]=[CH:8][CH:9]=2.[Cl:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20](Cl)=[O:21]>>[Cl:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]([C:8]1[CH:9]=[C:10]2[C:5]3=[C:6]([CH2:11][CH2:12][C:13](=[O:14])[N:4]3[CH2:3][CH2:2][CH2:1]2)[CH:7]=1)=[O:21]

Komponenten

3

Edukt 2

HCID 740895-Chlorovaleryl chlorideHCID 136945641,2,6,7-tetrahydro-5H-pyrido[3,2,1-ij]quinolin-3-one

Produkt 1

HCID 218872599-(5-chloropentanoyl)-1,2,6,7-tetrahydropyrido[3,2,1-ij]quinolin-3(5H)-one

Versuchsvorschrift

Using 2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one and 5-chlorovaleryl chloride according to the same method as that of Reference Example 1, the title compound (3.53 g) was obtained as colorless crystals, having a melting point of 83-84° C.

Quellen und Nachweise

ORD-Eintrag
ord-63ff60812e0e4418899874467087897a
Quelldatensatz
uspto-grants-2008_12
Patentnummer
US07462628B2

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