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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2375426Erstellt: 25. Oktober 2026

4-Amino-2,6-dibromophenol → HCID 69274007, Verbindung

https://huagongshe.com/reaction/2375426

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-Amino-2,6-dibromophenolHCID 69107—
EduktEthyl 2-acetyl-4-oxovalerateHCID 3084847—
LösungsmittelEthanolHCID 702—
ProduktHCID 69274007HCID 69274007—

Reaktionsschritte

Utilizing the procedure outlined in Example 85, ethyl 2-acetyl-4-oxopentanoate (6.37 g, 34.2 mmol) was dissolved in 20 mL of EtOH. 2,6-dibromo-4-aminophenol (11.6g, 34.2mmol) were reacted to afford ethyl 1-(3,5-dibromo-4-hydroxyphenyl)-2,5-dimethyl-1H-pyrrole-3-carboxylate was taken on without further purification. MS (ESI) 418 (M+H)+.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07465730B2
Quelldatensatzuspto-grants-2008_12
ORD IDord-d3768bf0effa473a8e30a37b8c51e892
Quellennotizuspto-grants-2008_12