Oxalic Acid → Carbonate oxalate

HRID 2377168

Reaktionsgleichung

Reaktionsgleichung von HRID 2377168
[C:1](=[O:4])([O-:3])[O-:2].[C:5]([OH:10])(=[O:9])[C:6]([OH:8])=[O:7]>C(OCC)(=O)C>[C:5]([OH:10])(=[O:9])[C:6]([OH:8])=[O:7].[C:1](=[O:2])([OH:4])[OH:3]

Komponenten

4

Edukt 2

HCID 971Oxalic AcidHCID 19660Carbonate Ion

Produkt 1

HCID 88099579Carbonate oxalate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8857Ethyl AcetateLösungsmittel2×

Versuchsvorschrift

In 7 mL of ethyl acetate was dissolved 0.31 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate, and to the solution was added a solution of 0.10 g of oxalic acid in 1 mL of ethyl acetate, after which the resulting mixture was stirred at room temperature. The crystals precipitated were collected by filtration to obtain 0.34 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate oxalate.

Aufarbeitung

  1. customThe crystals precipitated
  2. filtrationwere collected by filtration

Quellen und Nachweise

ORD-Eintrag
ord-b32e6c8bb44b4a0692fc1a911c2b56bc
Quelldatensatz
uspto-grants-2008_12
Patentnummer
US07468443B2

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