HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Methyl-2-cyclohexen-1-one → 3-Methyl-2-cyclohexen-1-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Methyl-2-cyclohexen-1-one | HCID 14511 | — |
| Edukt | HCID 178418373 | HCID 178418373 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 3-Methyl-2-cyclohexen-1-one | HCID 14511 | — |
| Produkt | Cyclohexanone, 3,3-dimethyl- | HCID 76322 | — |
Reaktionsschritte
First, 3-methyl-cyclohexenone was prepared in accordance with the procedures of Jirgensons et. al., Euro. J. Med. Chem. 35 (2000) 555-565. Then, 3-methyl-cyclohexenone was reacted with methyl magnesium iodide in the presence of cuprous chloride in diethyl ether to obtain the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08642603B2 |
| Quelldatensatz | uspto-grants-2014_02 |
| ORD ID | ord-f2ed5d56b2764e25bcbeb6e69c3a3e53 |
| Quellennotiz | uspto-grants-2014_02 |