Hydrochloric Acid → 2-Hydroxy-6-vinylbenzoic acid

HRID 2379279Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2379279
[OH:1][C:2]1[CH:12]=[CH:11][CH:10]=[C:9]([CH:13]=[CH2:14])[C:3]=1[C:4]([O:6]CC)=[O:5].[OH-].[Na+].Cl>CO>[OH:1][C:2]1[CH:12]=[CH:11][CH:10]=[C:9]([CH:13]=[CH2:14])[C:3]=1[C:4]([OH:6])=[O:5]

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 14798Sodium HydroxideHCID 15008897Ethyl 2-hydroxy-6-vinylbenzoate

Produkt 1

HCID 150088992-Hydroxy-6-vinylbenzoic acid

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

A solution of 3 g of ethyl 2-hydroxy-6-vinylbenzoate (see Example 1a), 150 ml of methanol and 45 ml of 10% by weight sodium hydroxide solution was boiled for 8 h. It was then poured into ice-water at pH 1 (hydrochloric acid) and extracted with ethyl acetate, and the solution was dried over sodium sulfate and evaporated under reduced pressure.

Aufarbeitung

  1. extractionextracted with ethyl acetate
  2. dry with materialthe solution was dried over sodium sulfate
  3. customevaporated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-e5cfc41b0b734c8db5bcdfbd9e47a93a
Quelldatensatz
uspto-grants-1994_11
Patentnummer
US05360913

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