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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2379300Erstellt: 25. Oktober 2026

Dichlorodimethylsilane → di(1H-inden-1-yl)dimethylsilane

https://huagongshe.com/reaction/2379300

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktDichlorodimethylsilaneHCID 6398—
EduktIndeneHCID 7219—
EduktButyllithiumHCID 178418339—
EduktHCID 178506815HCID 178506815—
Produktdi(1H-inden-1-yl)dimethylsilaneHCID 59942971%

Reaktionsschritte

In detail, in Japanese Patent Laid-Open Publication No. 221285/1990 for example, a solution of an indenyl lithium salt prepared from indene and n-butyllithium is slowly added to a dimethyldichlorosilane solution, and they are reacted with each other overnight to obtain dimethyldi(1-indenyl)silane in a 71% yield. In Japanese Patent Laid-Open Publication No. 268307/1992, dimethyldi (2-methyl-1-indenyl) silane is obtained in a 16% yield in a manner similar to the above.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05360921
Quelldatensatzuspto-grants-1994_11
ORD IDord-ce9b78dae72b4ddc992262c705339d43
Quellennotizuspto-grants-1994_11