HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → N-decyl galactosylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Decylamine | HCID 8916 | — |
| Edukt | beta-D-Galactopyranose | HCID 439353 | — |
| Lösungsmittel | Diethyl ether methanol | HCID 21864698 | — |
| Produkt | N-decyl galactosylamine | HCID 18656111 | 90% |
Reaktionsschritte
β-D-galactose (10 g, 1 eq), decylamine (8.7 g, 1 eq), and water (2 g, 3eq) were heated in a reaction flask for 20 min at 80° C. Methanol/ethyl ether (50 v/50 v) was added, the product was filtered, washed with ethyl ether (2×50 ml) and dried, to give a 90% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05362480 |
| Quelldatensatz | uspto-grants-1994_11 |
| ORD ID | ord-159b09309746474bb577eeb0211f48a2 |
| Quellennotiz | uspto-grants-1994_11 |