Ethionamide → HCID 22249370, Verbindung
Reaktionsgleichung
[CH3:1][CH2:2][C:3]1[CH:8]=[C:7]([C:9]([NH2:11])=S)[CH:6]=[CH:5][N:4]=1>CO.[Ni]>[CH2:2]([C:3]1[CH:8]=[C:7]([CH2:9][NH2:11])[CH:6]=[CH:5][N:4]=1)[CH3:1]Komponenten
4
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
To a solution of 2-ethyl-4-thiopyridylamide (10 g) in MeOH (250 ml) was added Raney 2800 Nickel (5 g, Aldrich) in one portion. The mixture was stirred at RT for 2 days then at 60° C. for 16 h. The mixture was filtered, concentrated to provide the desired compound.
Aufarbeitung
- waitat 60° C. for 16 h
- filtrationThe mixture was filtered
- concentrationconcentrated
Quellen und Nachweise
- ORD-Eintrag
- ord-1f1a9a1d4a0a48b9962f5fc0ecdccfd1
- Quelldatensatz
- uspto-grants-2014_02
- Patentnummer
- US08642624B2
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