Ethylenediamine → N~1~-(Pyridin-2-yl)ethane-1,2-diamine

HRID 238498

Reaktionsgleichung

Reaktionsgleichung von HRID 238498
[CH2:1]([NH2:4])[CH2:2][NH2:3].F[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][N:7]=1>>[N:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=1[NH:3][CH2:2][CH2:1][NH2:4]

Komponenten

3

Edukt 2

HCID 3301EthylenediamineHCID 97462-Fluoropyridine

Produkt 1

HCID 410428N~1~-(Pyridin-2-yl)ethane-1,2-diamine

Versuchsvorschrift

Ethylenediamine (6 g, 0.1 mol) and 2-fluoropyridine (10 g, 0.1 mol) were heated neat at 120° C. overnight. The reaction was cooled and the residue was used in next step without further purification.

Aufarbeitung

  1. temperatureThe reaction was cooled
  2. customthe residue was used in next step without further purification

Quellen und Nachweise

ORD-Eintrag
ord-d13c71bd5af9458eb262afc0d4dc0739
Quelldatensatz
uspto-grants-2014_02
Patentnummer
US08642624B2

Verknüpfte Notizen

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