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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2393653Erstellt: 23. Oktober 2026

Acetic Anhydride → HCID 136381103, Verbindung

https://huagongshe.com/de/reaction/2393653

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetic AnhydrideHCID 7918—
Edukt(R)-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl)-ornithinamideHCID 136381090—
LösungsmittelAcetic AcidHCID 176—
ProduktHCID 136381103HCID 136381103—

Reaktionsbedingungen

Temperatur50 °C

Reaktionsschritte

0.3 g (0.925 mMol) of (R)-N5 -[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide were dissolved in 3 ml of glacial acetic acid and after the addition of 3 ml (0.032 Mol) of acetic anhydride the mixture was heated to a reaction temperature of 50° C. for 30 minutes. The product remaining after the volatile components had evaporated off was further processed without purification.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05807875
Quelldatensatzuspto-grants-1998_09
ORD IDord-31ea9a0506fa40a8941c09e0e2b196c5
Quellennotizuspto-grants-1998_09