Thionyl Chloride → HCID 18974240, Verbindung

HRID 2394516Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2394516
[CH2:1]([O:7][C:8]1[CH:16]=[CH:15][C:11]([C:12](O)=[O:13])=[CH:10][CH:9]=1)[CH2:2][CH2:3][CH2:4][CH:5]=[CH2:6].S(Cl)([Cl:19])=O>N1C=CC=CC=1>[CH2:1]([O:7][C:8]1[CH:16]=[CH:15][C:11]([C:12]([Cl:19])=[O:13])=[CH:10][CH:9]=1)[CH2:2][CH2:3][CH2:4][CH:5]=[CH2:6]

Komponenten

4

Edukt 2

HCID 24386Thionyl ChlorideHCID 11148720Benzoic acid, 4-(5-hexenyloxy)-

Produkt 1

HCID 18974240HCID 18974240, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1049PyridineKatalysator

Versuchsvorschrift

The 4-(5-hexenyloxy)benzoic acid 10 g (0.046 mol) was reflux with thionyl chloride (5.4 mL, 0.069 mol) and several drops of pyridine for 8 hours. The excess thionyl chloride was removed in vacuo leaving 4-(5-hexenyl-oxy)benzoyl chloride as a clear liquid at 25° C. This acid chloride was used without further purification.

Aufarbeitung

  1. customThe excess thionyl chloride was removed in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-2dbaf929f41346db97059ae934eabcf9
Quelldatensatz
uspto-grants-1998_09
Patentnummer
US05811504

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