HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(2-Benzothiazol-2-ylthio)aniline → 1-[4-(2-Benzothiazolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(2-Benzothiazol-2-ylthio)aniline | HCID 117610 | — |
| Edukt | 1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene | HCID 520026 | — |
| Produkt | 1-[4-(2-Benzothiazolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea | HCID 18971677 | — |
Reaktionsschritte
2-(4-Aminophenylthio)benzothiazole (10.0 mmoles, 2.6 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate 10.0 mmoles, 2.4 g) were reacted according to procedure C to yield of the title compound, 1.5 g, 30%. Mass Spec (FD) 495. Calculated for C21H13ClF3 N3S3 : C, 50.85H, 2.64N, 8.47. Found: C, 51.02; H, 2.71; N, 8.31.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05814646 |
| Quelldatensatz | uspto-grants-1998_09 |
| ORD ID | ord-3dec1a035fb04497968cce9aaa1d4d2f |
| Quellennotiz | uspto-grants-1998_09 |