Ethanol → Ethyl sulfoacetate

HRID 2396092

Reaktionsgleichung

Reaktionsgleichung von HRID 2396092
[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH3:9][CH2:10]O>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

Komponenten

3

Edukt 2

HCID 702EthanolHCID 31257Sulfoacetic acid

Produkt 1

HCID 12216623Ethyl sulfoacetate

Versuchsvorschrift

Sulfoacetic acid (52 g, 371 mM) and EtOH (500 mL) were heated under reflux for 20 hours. The reaction mixture was cooled, and the excess ethanol was removed under vacuum to give ethyl sulfoacetate.

Aufarbeitung

  1. temperatureunder reflux for 20 hours
  2. temperatureThe reaction mixture was cooled
  3. customthe excess ethanol was removed under vacuum

Quellen und Nachweise

ORD-Eintrag
ord-292b72945d0e454c82fdb19175274c63
Quelldatensatz
uspto-grants-1996_02
Patentnummer
US05491170

Verknüpfte Notizen

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