HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,4-Dichloro-6-nitroaniline → 10,12-Dichlorodibenzo[a,c]phenazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,4-Dichloro-6-nitroaniline | HCID 75893 | — |
| Edukt | 1,2-Phenanthrenedione | HCID 3080566 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | 10,12-Dichlorodibenzo[a,c]phenazine | HCID 21391728 | 81% |
Reaktionsschritte
When 0.12 mole each of 2,4-dichloro-6-nitroaniline and phenanthrenequinone were reacted by the method of Example 1, 24 g. (81 percent yield) of 10,12-dichlorodibenzo[a,c]phenazine, mp = 221°-222° C. (acetone), were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04024142 |
| Quelldatensatz | uspto-grants-1977_05 |
| ORD ID | ord-c685a2d995134aac9264c610b96024d7 |
| Quellennotiz | uspto-grants-1977_05 |