HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → Hydrochloric Acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Gabapentin | HCID 3446 | — |
| Produkt | Hydrochloric Acid | HCID 313 | — |
| Produkt | Ethyl 2-[1-(aminomethyl)cyclohexyl]acetate | HCID 15512485 | — |
Reaktionsschritte
10 g. of the 1-aminomethyl-1-cyclohexane-acetic acid, prepared according to Example 1, are dissolved in 50 ml. anhydrous ethanol and saturated at 0° C. with gaseous hydrogen chloride. The reaction mixture is left to stand overnight at ambient temperature, then evaporated in a vacuum and the residue recrystallised from ethanol/ether. Ethyl 1-aminomethyl-1-cyclohexane-acetate is obtained in the form of its hydrochloride; m.p. 161°-163° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04024175 |
| Quelldatensatz | uspto-grants-1977_05 |
| ORD ID | ord-5b486aab7e8f4d858162b956a36109a8 |
| Quellennotiz | uspto-grants-1977_05 |