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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2398120Erstellt: 27. Oktober 2026

Hydrochloric Acid → Hydrochloric Acid

https://huagongshe.com/reaction/2398120

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrochloric AcidHCID 313—
EduktEthanolHCID 702—
EduktGabapentinHCID 3446—
ProduktHydrochloric AcidHCID 313—
ProduktEthyl 2-[1-(aminomethyl)cyclohexyl]acetateHCID 15512485—

Reaktionsschritte

10 g. of the 1-aminomethyl-1-cyclohexane-acetic acid, prepared according to Example 1, are dissolved in 50 ml. anhydrous ethanol and saturated at 0° C. with gaseous hydrogen chloride. The reaction mixture is left to stand overnight at ambient temperature, then evaporated in a vacuum and the residue recrystallised from ethanol/ether. Ethyl 1-aminomethyl-1-cyclohexane-acetate is obtained in the form of its hydrochloride; m.p. 161°-163° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04024175
Quelldatensatzuspto-grants-1977_05
ORD IDord-5b486aab7e8f4d858162b956a36109a8
Quellennotizuspto-grants-1977_05