HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(N-Propionylaniline)piperidine → N-(2,6-dimethylphenoxyethyl)-4-(N'-phenyl-N'-propylamino)-piperidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(N-Propionylaniline)piperidine | HCID 259381 | — |
| Edukt | 2-(2-Bromoethoxy)-1,3-dimethylbenzene | HCID 2452208 | — |
| Produkt | N-(2,6-dimethylphenoxyethyl)-4-(N'-phenyl-N'-propylamino)-piperidine | HCID 54259289 | 79,7% |
Reaktionsschritte
Using the procedure described in Example I and starting from 12.7 g (2,6-dimethylphenoxyethyl) bromide and 12.8 g 4-(N'-phenyl-N'-propionylamino)-piperidine, 16.1 g of the title product are obtained melting at 82° after recrystallization from hexane. Mixing the compound with 4-(N'-phenyl-N'-propionylamino)-piperidine depresses the melting point.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04027028 |
| Quelldatensatz | uspto-grants-1977_05 |
| ORD ID | ord-37cb28822f0a47079faff14e341d37ae |
| Quellennotiz | uspto-grants-1977_05 |