HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanol → 3-methoxy-9-oxo-9H-indeno[1,2-b]pyrazine-2-carbonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanol | HCID 887 | — |
| Edukt | 9-oxo-9H-indeno(1,2-b)pyrazine-2,3-dicarbonitrile | HCID 292929 | — |
| Produkt | 3-methoxy-9-oxo-9H-indeno[1,2-b]pyrazine-2-carbonitrile | HCID 16065353 | 126,5% |
Reaktionsschritte
To a suspension of 1 (1.10 g, 4.7 mmol) in MeOH (47 ml) sodium (110 mg) was added and the mixture was stirred at room temperature for 16 hours. The precipitate was filtered, washed with EtOH and dried under vacuum, yielding 3 (1.03 g, 93%) as yellow-green solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08648076B2 |
| Quelldatensatz | uspto-grants-2014_02 |
| ORD ID | ord-b40012b19977406f87d5a10b4b6e4989 |
| Quellennotiz | uspto-grants-2014_02 |