Hydrochloric Acid → HCID 178510555, Verbindung

Beteiligte Stoffe

Reaktionsschritte

A suspension of 1 (5.66 g, 24.3 mmol) in aqueous NaOH (2% w/v, 81 ml) was stirred at room temperature for 16 hours. The mixture was acidified with 3N HCl to pH 1, the precipitate was collected by filtration, washed with water and dried under vacuum, affording 6 (4.88 g, 90%) as light brown solid.

Herkunft & Nachweise