Formamide → HCID 178518064, Verbindung
Reaktionsgleichung
C([O:3][C:4]([C:6]1[C:7]2[CH2:15][CH2:14][CH2:13][CH2:12][C:8]=2[S:9][C:10]=1[NH2:11])=O)C.[CH:16]([NH2:18])=O>>[N:11]1[C:10]2[S:9][C:8]3[CH2:12][CH2:13][CH2:14][CH2:15][C:7]=3[C:6]=2[C:4]([OH:3])=[N:18][CH:16]=1Komponenten
3
Versuchsvorschrift
A solution of 10 millimol IV in 15 milliliter formamide was stirred at 100° C. for 3 hours then cooled down to room temperature. The reaction mixture was poured onto crushed ice with continuous stirring then collected by filtration. The product was washed with water and n-hexane, then dried.
Aufarbeitung
- additionThe reaction mixture was poured
- customonto crushed ice
- filtrationthen collected by filtration
- washThe product was washed with water and n-hexane
- customdried
Quellen und Nachweise
- ORD-Eintrag
- ord-f0bb1876f5634d4286cc669c9e7cfd02
- Quelldatensatz
- uspto-grants-2014_08
- Patentnummer
- US08802849B2
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