N-methyl-N-phenyl-hydrazine → 5-(4-chloro-phenyl)-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid N'-methyl-N'-phenyl-hydrazide
Reaktionsgleichung
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:9]=[C:10]([C:20]([OH:22])=O)[CH:11]=[N:12][C:13]=2[O:14][CH2:15][C:16]([F:19])([F:18])[F:17])=[CH:4][CH:3]=1.[CH3:23][N:24]([C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)[NH2:25]>>[CH3:23][N:24]([C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)[NH:25][C:20]([C:10]1[CH:11]=[N:12][C:13]([O:14][CH2:15][C:16]([F:17])([F:18])[F:19])=[C:8]([C:5]2[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][CH:6]=2)[CH:9]=1)=[O:22]Komponenten
3
Versuchsvorschrift
The title compound was synthesized in analogy to Example 1 using 5-(4-chlorophenyl)-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid (CAN 1018782-82-5) and 1-methyl-1-phenyl-hydrazine (CAN 618-40-6) as starting materials; MS (EI) 436.3 (M+H)+.
Quellen und Nachweise
- ORD-Eintrag
- ord-7c8b2c96f5f84582ab96174c654b13c2
- Quelldatensatz
- uspto-grants-2014_02