N-methyl-N-phenyl-hydrazine → 5-cyclohexyl-N'-methyl-N'-phenyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide

HRID 240710

Reaktionsgleichung

Reaktionsgleichung von HRID 240710
[CH:1]1([C:7]2[CH:8]=[C:9]([C:19](O)=[O:20])[CH:10]=[N:11][C:12]=2[O:13][CH2:14][C:15]([F:18])([F:17])[F:16])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH3:22][N:23]([C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1)[NH2:24]>>[CH:1]1([C:7]2[CH:8]=[C:9]([C:19]([NH:24][N:23]([CH3:22])[C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)=[O:20])[CH:10]=[N:11][C:12]=2[O:13][CH2:14][C:15]([F:17])([F:16])[F:18])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Komponenten

3

Edukt 2

HCID 36299N-methyl-N-phenyl-hydrazineHCID 712939525-Cyclohexyl-6-(2,2,2-trifluoroethoxy)nicotinic acid

Produkt 1

HCID 712943645-cyclohexyl-N'-methyl-N'-phenyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide

Versuchsvorschrift

The title compound was synthesized in analogy to Example 1 using 5-cyclohexyl-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid (example 12c) and 1-methyl-1-phenyl-hydrazine (CAN 618-40-6) as starting materials; MS (EI) 408.4 (M+H)+.

Quellen und Nachweise

ORD-Eintrag
ord-a07d4e0898c243a48111d4ed2a414b8b
Quelldatensatz
uspto-grants-2014_02
Patentnummer
US08648099B2

Verknüpfte Notizen

Wird geladen…