Hydrogen Bromide → Hydrogen Bromide
Reaktionsgleichung
C[O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH:9]1[CH2:14][CH2:13][CH2:12][NH:11][CH2:10]1.Cl.[BrH:16]>>[BrH:16].[NH:11]1[CH2:12][CH2:13][CH2:14][CH:9]([C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[OH:2])[CH2:10]1Komponenten
5
Versuchsvorschrift
HBr was prepared by heating 3-(2-methoxyphenyl)piperidine.HCl (46 mg, 0.20 mmol) with 48% HBr in a microwave reactor at 120° C. for one hour. After evaporation, 61 mg of the title compound was obtained.
Aufarbeitung
- customAfter evaporation
Quellen und Nachweise
- ORD-Eintrag
- ord-a6d93d1dbd8c4534baea82c3619c9ffa
- Quelldatensatz
- uspto-grants-2014_08
- Patentnummer
- US08809536B2
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