Benzyl azide → 1-Benzyl-5-methyl-4-(tributylstannyl)-1H-1,2,3-triazole

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

Tributyl(1-propynyl)tin (3.87 g, 11.8 mmol) and benzyl azide (2.2 mL, 17.6 mmol) were combined and heated to 150° C. overnight. The mixture was purified by silica gel chromatography eluting with a gradient of 5-40% ethyl acetate in hexanes to afford the title compound. MS (ESI+) m/z 464.2 (M+H)+.

Herkunft & Nachweise