HCID 20474893, Verbindung → HCID 58504163, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[S:6][C:5]([C:7]([OH:9])=O)=[C:4]([CH3:10])[C:3]=1[C:11]#[N:12].[C:13]1([C:19]2[CH:23]=[C:22]([CH2:24][N:25]3[CH2:30][CH2:29][CH:28]([CH2:31][NH2:32])[CH2:27][CH2:26]3)[O:21][N:20]=2)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[NH2:1][C:2]1[S:6][C:5]([C:7]([NH:32][CH2:31][CH:28]2[CH2:27][CH2:26][N:25]([CH2:24][C:22]3[O:21][N:20]=[C:19]([C:13]4[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=4)[CH:23]=3)[CH2:30][CH2:29]2)=[O:9])=[C:4]([CH3:10])[C:3]=1[C:11]#[N:12]Komponenten
3
Versuchsvorschrift
According to the same procedure described in Example 225, using the compound prepared in Example 227 instead of 4-amino-5-cyano-6-ethoxypicolinic acid, and using the compound prepared in Example 9 instead of tert-butyl 4-(aminomethyl)piperidine-1-carboxylate, the title compound having the following physical data was obtained.
Quellen und Nachweise
- ORD-Eintrag
- ord-655448dd472c49b7b22fd2c276505b99
- Quelldatensatz
- uspto-grants-2014_08
- Patentnummer