tert-Octylamine → HCID 86656469, Verbindung

Reaktionsgleichung

[N:1]([CH2:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][CH:10]=1)=[C:2]=[S:3].[C:11]([NH2:19])([CH2:14][C:15]([CH3:18])([CH3:17])[CH3:16])([CH3:13])[CH3:12]>>[C:11]([NH:19][C:2]([NH:1][CH2:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][CH:10]=1)=[S:3])([CH2:14][C:15]([CH3:18])([CH3:17])[CH3:16])([CH3:13])[CH3:12]

Komponenten

Edukt 2

HCID 61017tert-Octylamine

HCID 101763092-(2-Isothiocyanatoethyl)thiophene

Produkt 1

HCID 86656469HCID 86656469, VerbindungAusbeute 83 %

Versuchsvorschrift

The procedure of step (1-1) of Example 1 was repeated except for using the compound obtained in step (2-1) (2.5 g, 15.0 mmol) and t-octyl amine (1.6 mL, 10.2 mmol), to obtain the title compound (2.5 g, 83%).

Quellen und Nachweise

ORD-Eintrag: ord-c833821c4062406bbd394a19d3e2b44e
Quelldatensatz: uspto-grants-2014_02
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08648111B2

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