HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Methoxyaniline → N-(2-methoxyphenyl)-3-nitrobenzenesulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Methoxyaniline | HCID 7000 | — |
| Edukt | 3-Nitrobenzenesulfonyl chloride | HCID 8476 | — |
| Produkt | N-(2-methoxyphenyl)-3-nitrobenzenesulfonamide | HCID 2834884 | 89,5% |
Reaktionsschritte
Using o-anisidine (1.0 ml, 8.55 mmol) and 3-nitrobenzenesulfonyl chloride (1.95 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.36 g (89.5%) of the title compound in the form of light yellow needle crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05728835 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-df69311069264a20a142aa147b4fbb47 |
| Quellennotiz | uspto-grants-1998_03 |