Methyl iodide → 3,5-Dimethyl-2,4-Imidazolidinedione

Reaktionsgleichung

[CH3:1][CH:2]1[NH:6][C:5](=[O:7])[NH:4][C:3]1=[O:8].[CH3:9]I>>[CH3:9][N:4]1[C:3](=[O:8])[CH:2]([CH3:1])[NH:6][C:5]1=[O:7]

Komponenten

Edukt 2

HCID 6328Methyl iodide

HCID 692165-Methylhydantoin

Produkt 1

HCID 101540613,5-Dimethyl-2,4-Imidazolidinedione

Versuchsvorschrift

Using 5-methylimidazolidine-2,4-dione (1.00 g) and methyl iodide (0.57 mL) and by the reaction and treatment in the same manner as in Preparation Example 214, the title compound (1.66 g, containing DMF) was obtained.

Aufarbeitung

customby the reaction and treatment in the same manner
customas in Preparation Example 214

Quellen und Nachweise

ORD-Eintrag: ord-6a391b4510b048bf8b2cb1df12641ef4
Quelldatensatz: uspto-grants-2014_08
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08816079B2

Notizen zur Reaktion

Wird geladen…