HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → HCID 54446174, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Allyltriphenylphosphonium bromide | HCID 197740 | — |
| Edukt | 2-Fluoro-1-trityl-1H-imidazole-4-carbaldehyde | HCID 53779028 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 54446174 | HCID 54446174 | — |
Reaktionsschritte
2-Fluoro-4-formyl-1-triphenylmethylimidazole was reacted with allyl triphenyl phosphonium bromide in CH2Cl2 in the presence of aqueous NaOH to give 4-(buta-1,3-dienyl)-2-fluoro-1-triphenylmethylimidazole having the following n.m.r. spectrum in CDCl3 : 5.06-5.39 (m, 2H); 5.87 (d, 1H); 6.06 (dd, 1H); 6.49 (s, 1H); 7.51 and 7.7 (d of t, 3H); 7.08-7.44 (br, 15H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04492692 |
| Quelldatensatz | uspto-grants-1985_01 |
| ORD ID | ord-7a76a7f448324455a663cb68ee5447d0 |
| Quellennotiz | uspto-grants-1985_01 |