4-Methoxybenzaldehyde → HCID 54069780, Verbindung
Reaktionsgleichung
[NH2:1][CH2:2][P:3](=[O:10])([O:7][CH2:8][CH3:9])[O:4][CH2:5][CH3:6].[CH3:11][O:12][C:13]1[CH:20]=[CH:19][C:16]([CH:17]=O)=[CH:15][CH:14]=1>>[CH3:11][O:12][C:13]1[CH:20]=[CH:19][C:16]([CH:17]=[N:1][CH2:2][P:3](=[O:10])([O:7][CH2:8][CH3:9])[O:4][CH2:5][CH3:6])=[CH:15][CH:14]=1Komponenten
3
Versuchsvorschrift
Starting from 16.7 g. (0.1 mol) diethyl aminomethylphosphonate and 13.6 g. (0.1 mol) p-methoxybenzaldehyde and following the procedure described in Example 1, 28.5 g. (yield: 100%) of the desired product are obtained in the form of a yellow oil.
Quellen und Nachweise
- ORD-Eintrag
- ord-04eb668a816d407780fc670af25be8b7
- Quelldatensatz
- uspto-grants-1985_01
- Patentnummer
- US04493931
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