HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → Methane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Ethanol | HCID 702 | — |
| Edukt | 4-(Dimethylamino)Benzaldehyde | HCID 7479 | — |
| Edukt | 1H-Indole, 1-ethyl-2-methyl- | HCID 170432 | — |
| Edukt | Sodium p-toluenesulfinate | HCID 2723791 | — |
| Produkt | Methane | HCID 297 | — |
| Produkt | [(4-Dimethylaminophenyl)(1-ethyl-2-methyl-3-indolyl)(4-methylphenylsulfonyl)]methane | HCID 20184815 | — |
Reaktionsschritte
Proceeding in a manner similar to that described in Example 1 above substituting for ethyl alcohol and the concentrated hydrochloric acid the appropriate reaction medium and the appropriate catalyst listed in Examples 58-82 of Table A hereinbelow, 4-dimethylaminobenzaldehyde, sodium p-toluenesulfinate and 1-ethyl-2-methylindole were interacted at the indicated temperature to obtain a methane of Formula II wherein R=4--CH3 ; R1 =CH3 ; R3 =R5 =H; R6 =N(CH3)2. A toluene or acetone solution of the product from Examples 58-82 contacted with silica gel developed at blue-red colored image.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04494989 |
| Quelldatensatz | uspto-grants-1985_01 |
| ORD ID | ord-9844834c967443a9a82115fbb841dac2 |
| Quellennotiz | uspto-grants-1985_01 |