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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2412822Erstellt: 26. Oktober 2026

Hydrochloric Acid → Methane

https://huagongshe.com/reaction/2412822

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrochloric AcidHCID 313—
EduktEthanolHCID 702—
Edukt4-(Dimethylamino)BenzaldehydeHCID 7479—
Edukt1H-Indole, 1-ethyl-2-methyl-HCID 170432—
EduktSodium p-toluenesulfinateHCID 2723791—
ProduktMethaneHCID 297—
Produkt[(4-Dimethylaminophenyl)(1-ethyl-2-methyl-3-indolyl)(4-methylphenylsulfonyl)]methaneHCID 20184815—

Reaktionsschritte

Proceeding in a manner similar to that described in Example 1 above substituting for ethyl alcohol and the concentrated hydrochloric acid the appropriate reaction medium and the appropriate catalyst listed in Examples 58-82 of Table A hereinbelow, 4-dimethylaminobenzaldehyde, sodium p-toluenesulfinate and 1-ethyl-2-methylindole were interacted at the indicated temperature to obtain a methane of Formula II wherein R=4--CH3 ; R1 =CH3 ; R3 =R5 =H; R6 =N(CH3)2. A toluene or acetone solution of the product from Examples 58-82 contacted with silica gel developed at blue-red colored image.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04494989
Quelldatensatzuspto-grants-1985_01
ORD IDord-9844834c967443a9a82115fbb841dac2
Quellennotizuspto-grants-1985_01