m-Chloroperbenzoic acid → 3-methylsulfinyl-N'-sulfamoylpropanimidamide

Beteiligte Stoffe

Reaktionsschritte

A solution of commercial 80% pure m-chloroperbenzoic acid (5.4 g, 25 mmol) in chloroform (40 ml) was added dropwise to a solution of N-sulfamyl-3-(methylthio)propionamidine (4.94 g, 25 mmol) in methanol (50 ml) at room temperature. After stirring for two hours, the product was collected by filtration, analytically pure, to give 4.44 g, mp 141°-144°.

Herkunft & Nachweise