2-Amino-2-methyl-1,3-propanediol → [2-(Chrysen-3-ylmethylamino)-3-hydroxy-2-methylpropyl] methanesulfonate

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	2-Amino-2-methyl-1,3-propanediol	HCID 1531	—
Edukt	Chrysene-3-carbaldehyde	HCID 15599326	—
Edukt	2-((6-Chrysenylmethyl)amino)-2-methyl-1,3-propanediol methanesulfonate	HCID 54096087	—
Produkt	[2-(Chrysen-3-ylmethylamino)-3-hydroxy-2-methylpropyl] methanesulfonate	HCID 54185837	—

Reaktionsschritte

Using the reductive amination procedure outlined in 1C, chrysene-3-carbaldehyde (19G) and 2-amino-2-methyl-1,3-propanediol (Aldrich) gave 2-((3-chrysenylmethyl)amino)-2-methyl-1,3-propanediol methanesulfonate mp 180°-182° (dec), (EtOH/Et2O), (C, H, N, S).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US04719046
Quelldatensatz	uspto-grants-1988_01
ORD ID	ord-75276da1821241cd89398487bea062d2
Quellennotiz	uspto-grants-1988_01