HCID 22640158, Verbindung → 1-Biphenyl-4-yl-piperazine

HRID 2415143Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2415143
C([N:8]1[CH2:13][CH2:12][N:11]([C:14]2[CH:19]=[CH:18][C:17]([C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)=[CH:16][CH:15]=2)[CH2:10][CH2:9]1)C1C=CC=CC=1>CO.[OH-].[Pd+2].[OH-]>[C:17]1([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:18]=[CH:19][C:14]([N:11]2[CH2:10][CH2:9][NH:8][CH2:13][CH2:12]2)=[CH:15][CH:16]=1

Komponenten

4

Edukt 1

HCID 22640158HCID 22640158, Verbindung

Produkt 1

HCID 27355131-Biphenyl-4-yl-piperazine

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 9942167Palladium hydroxideKatalysatorHCID 887MethanolLösungsmittel

Versuchsvorschrift

A suspension of 12.45 g (0.037 mol) of 1-benzyl-4-biphenyl-4-yl-piperazine and 4 g of palladium hydroxide in 360 ml of methanol is stirred for 6 hours at ambient temperature in a Parr apparatus under a hydrogen pressure of 50 psi. The catalyst is separated off and the filtrate is evaporated down.

Aufarbeitung

  1. customThe catalyst is separated off
  2. customthe filtrate is evaporated down

Quellen und Nachweise

ORD-Eintrag
ord-59a29e27e8a44363bf5f47598bfd299e
Quelldatensatz
uspto-grants-2004_11
Patentnummer
US06818644B1

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