HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3-Benzenediamine, N1,N1-dimethyl-, hydrochloride (1:2) → 4-chloro-N-(3-dimethylaminophenyl)-3-(4-propylbenzamido)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3-Benzenediamine, N1,N1-dimethyl-, hydrochloride (1:2) | HCID 77124 | — |
| Edukt | 4-Chloro-3-(4-propylbenzamido)benzoyl chloride | HCID 22636129 | — |
| Produkt | 4-chloro-N-(3-dimethylaminophenyl)-3-(4-propylbenzamido)benzamide | HCID 9889221 | — |
Reaktionsschritte
Using an analogous procedure to that described in Example 1, 4-chloro-3-(4-propylbenzamido)benzoyl chloride was reacted with 3-dimethylamino aniline dihydrochloride to give the title compound; NMR Spectrum: (DMSOd6) 0.9 (t, 3H), 1.18 (t, 2H), 1.69 (m, 2H), 2.99 (s, 6H), 7.0 (d, 1H), 7.2-7.5 (m, 4H) 7.64-7.8 (m, 3H), 7.84 (d, 1H), 8.0 (m, 2H), 8.19 (s, 1H); Mass Spectrum: M+H+ 436 and 438.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06821965B1 |
| Quelldatensatz | uspto-grants-2004_11 |
| ORD ID | ord-c3245b290fc54d88976e4a5631543b4a |
| Quellennotiz | uspto-grants-2004_11 |