Hydrochloric Acid → 2-Methyl-1-phenylpiperaZine hydrochloride

HRID 2416657Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2416657
[CH3:1][CH:2]1[N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH2:6][CH2:5][N:4](C(OC(C)(C)C)=O)[CH2:3]1.[ClH:21]>C(OCC)(=O)C>[ClH:21].[C:8]1([N:7]2[CH2:6][CH2:5][NH:4][CH2:3][CH:2]2[CH3:1])[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 226330714-Boc-2-methyl-1-phenylpiperazine

Produkt 1

HCID 226330592-Methyl-1-phenylpiperaZine hydrochloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8857Ethyl AcetateLösungsmittel

Versuchsvorschrift

(±)-tert-Butyl 3-methyl-4-phenylpiperazine-1-carboxylate (142 mg) was dissolved in 4N hydrogen chloride in ethyl acetate (5 ml). After stirring for 15 minutes, the solvent was removed under reduced pressure to give the title compound as a slightly yellow solid.

Aufarbeitung

  1. customthe solvent was removed under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-bad87fa887ec45f383499b68be82f86c
Quelldatensatz
uspto-grants-2004_11
Patentnummer
US06825200B1

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