Reaktionsgleichung
[CH2:1]([OH:19])[CH2:2][CH2:3]CCCCCCCCCCCCCCC.C1(CN=C=O)C(CN=C=[O:29])=CC=CC=1.C(C(CO)(CO)CC)O.C1C=C(C[N:50]=[C:51]=[O:52])C=C(CN=C=O)C=1.C([O-])(=O)CCCCCCCCCCC.C([Sn+2]CCCC)CCC.C([O-])(=O)CCCCCCCCCCC.COC1C=CC(O)=CC=1>C1(C)C=CC=CC=1>[C:1]([OH:19])(=[O:29])[CH:2]=[CH2:3].[NH2:50][C:51]([O:19][CH2:1][CH3:2])=[O:52]Komponenten
Edukt 6
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Reaktionsbedingungen
- Temperatur
- 40 °C
Versuchsvorschrift
Into a flask similar to the flask in Synthesis Example 1 were charged 44.8 parts of toluene and 4.6 parts of stearyl alcohol (NAA-46), followed by heating of the mixture to 40° C. After the confirmation of thorough dissolution of stearyl alcohol, 50 parts of xylylene diisocyanate subjected to trimethylol-propane adduct modification (“TAKENATE D-110N” a trade name of Takeda Chemical Industries, Ltd., N.V.: 75, NCO %: 11.5) were charged and the mixture was heated to 70° C. After 30 minutes of the reaction at the same temperature, 0.02 parts of dibutyltin laurate were charged. After the mixture was maintained at the same temperature for 3 hours, 91.7 parts of polycaprolactone-modified hydroxyethyl acrylate (PLACCEL FA5), 0.02 parts of dibutyltin laurate, and 0.02 parts of hydroquinone monomethyl ether were charged. The mixture was maintained at 70° C. for 3 hours to complete the reaction, and 76.5 parts of toluene were added to obtain a urethane acrylate containing 50% by weight of solid.
Aufarbeitung
- customInto a flask similar to the flask in Synthesis Example 1
- addition: 75, NCO %: 11.5) were charged
- temperaturethe mixture was heated to 70° C
- additionwere charged
- temperatureAfter the mixture was maintained at the same temperature for 3 hours
- temperatureThe mixture was maintained at 70° C. for 3 hours
- additionwere added
Quellen und Nachweise
- ORD-Eintrag
- ord-17ebe6446b3942bdafa6a6bbfa6ea1a3
- Quelldatensatz
- uspto-grants-2004_11
- Patentnummer
- US06825243B2
Verknüpfte Notizen
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