Iron(2+) tetrafluoroborate--water (1/2/6) → Borate(1-), tetrafluoro-, iron(2+) (2:1)
Reaktionsgleichung
O.O.O.O.O.O.[F:7][B-:8]([F:11])([F:10])[F:9].[F:12][B-:13]([F:16])([F:15])[F:14].[Fe+2:17]>ClCCl>[F:7][B-:8]([F:11])([F:10])[F:9].[F:12][B-:13]([F:16])([F:15])[F:14].[Fe+2:17]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
To a suspension of iron(II) bis(tetrafluoroborate)hexahydrate (4.9 mg; 15 μmol) in dichloromethane was added a solution of h17 (5.0 mg; 14 μmol) in a few milliliters of dichloromethane. The solution turned from light yellow to dark orange with time within 18 hours. The solution was used as is in further polymerization study.
Aufarbeitung
- customwithin 18 hours
Quellen und Nachweise
- ORD-Eintrag
- ord-f952c70f2fbe46af861191f886200573
- Quelldatensatz
- uspto-grants-2004_11
- Patentnummer
- US06825356B2
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