3,4-Dichloroaniline → 2-(3,4-Dichloroanilino)-1H-benzimidazole

Reaktionsgleichung

Cl[C:2]1[NH:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[Cl:11][C:12]1[CH:13]=[C:14]([CH:16]=[CH:17][C:18]=1[Cl:19])[NH2:15]>>[N:6]1[C:5]2[CH:7]=[CH:8][CH:9]=[CH:10][C:4]=2[NH:3][C:2]=1[NH:15][C:14]1[CH:16]=[CH:17][C:18]([Cl:19])=[C:12]([Cl:11])[CH:13]=1

Komponenten

Edukt 2

HCID 72573,4-Dichloroaniline

HCID 785722-Chlorobenzimidazole

Produkt 1

HCID 9238632-(3,4-Dichloroanilino)-1H-benzimidazole

Versuchsvorschrift

The title compound was prepared from 2-chlorobenzimidazole and 3,4-dichloroaniline by Procedure A. The product was isolated by filtration to give the title compound as a hydrochloride salt (white solid, mp>270° C.). MS(ES+) m/z 278 (M+, 100).

Aufarbeitung

customThe product was isolated by filtration

Quellen und Nachweise

ORD-Eintrag: ord-8f3e400e18a04aaaa3dfb2ef67049778
Quelldatensatz: uspto-grants-2011_06
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07960561B2

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