Hydrochloric Acid → HCID 11851689, Verbindung
Reaktionsgleichung
[NH2:1][CH2:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][S:10]([CH3:13])(=[O:12])=[O:11])=[C:5]([I:14])[CH:4]=1.Cl.C1([O:22][C:23](=O)[NH:24][CH2:25][C:26]2[CH:31]=[CH:30][C:29]([C:32]([CH3:35])([CH3:34])[CH3:33])=[CH:28][CH:27]=2)C=CC=CC=1>>[C:32]([C:29]1[CH:30]=[CH:31][C:26]([CH2:25][NH:24][C:23](=[O:22])[NH:1][CH2:2][C:3]2[CH:8]=[CH:7][C:6]([NH:9][S:10]([CH3:13])(=[O:12])=[O:11])=[C:5]([I:14])[CH:4]=2)=[CH:27][CH:28]=1)([CH3:35])([CH3:33])[CH3:34]Komponenten
4
Versuchsvorschrift
N-(4-Aminomethyl-2-iodo-phenyl)-methanesulfonamide and HCl salt (297 mg, 0.820 mmol) were reacted with (4-t-butyl-benzyl)-carbamic acid phenyl ester following the general procedure to give a white solid (152 mg).
Quellen und Nachweise
- ORD-Eintrag
- ord-608be4d1f94e4bc68ea5ec8ae2c78c30