HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
6-Isocyanato-2,3-dihydro-1,4-benzodioxine → 1-Cyclopentyl-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-7-methoxy-1H-pyrimido[5,4-c]quinoline-2,4-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 6-Isocyanato-2,3-dihydro-1,4-benzodioxine | HCID 2776172 | — |
| Edukt | 4-Cyclopentylamino-8-methoxy-quinoline-3-carboxylic acid ethyl ester | HCID 67249718 | — |
| Produkt | 1-Cyclopentyl-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-7-methoxy-1H-pyrimido[5,4-c]quinoline-2,4-dione | HCID 58329469 | 40,4% |
Reaktionsschritte
1-Cyclopentyl-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-7-methoxy-1H-pyrimido[5,4-c]quinoline-2,4-dione (18 mg) was prepared from 4-cyclopentylamino-8-methoxy-quinoline-3-carboxylic acid ethyl ester (0.1 mmol) and 6-isocyanato-2,3-dihydro-benzo[1,4]dioxine (0.5 mmol) following general procedure C. LCMS: m/z 446 [M+1]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07964608B2 |
| Quelldatensatz | uspto-grants-2011_06 |
| ORD ID | ord-4e384f9e8d72480cb07846157fe08268 |
| Quellennotiz | uspto-grants-2011_06 |