HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2426746Erstellt: 26. Oktober 2026
Ethanol → 6-Methoxy-2',6'-dimethylbiphenyl-3-carbaldehyde
https://huagongshe.com/reaction/2426746
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | 2-Bromo-m-xylene | HCID 68471 | — |
| Edukt | 5-Formyl-2-methoxyphenylboronic acid | HCID 2734367 | — |
| Katalysator | HCID 178418397 | HCID 178418397 | — |
| Lösungsmittel | 1,2-Dimethoxyethane | HCID 8071 | — |
| Produkt | 6-Methoxy-2',6'-dimethylbiphenyl-3-carbaldehyde | HCID 57787305 | — |
Reaktionsschritte
In an atmosphere of nitrogen, tetrakis(triphenylphosphine)palladium was added to a mixture of 2-bromo-1,3-dimethylbenzene, (5-formyl-2-methoxyphenyl)boronic acid, a 1 M sodium carbonate aqueous solution, ethanol and dimethoxyethane, followed by stirring at 80° C. for 25 hours to obtain 6-methoxy-2′,6′-dimethylbiphenyl-3-carbaldehyde.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US07968552B2 |
|---|
| Quelldatensatz | uspto-grants-2011_06 |
|---|
| ORD ID | ord-10e8261531c149c8bb14835d0b23a899 |
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| Quellennotiz | uspto-grants-2011_06 |
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