HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Fluoroisatin → 5-fluoro-1,3-dihydro-2H-indol-2-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Fluoroisatin | HCID 236566 | — |
| Lösungsmittel | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Produkt | 5-fluoro-1,3-dihydro-2H-indol-2-one | HCID 3731012 | — |
Reaktionsschritte
5-Fluoroisatin (8.2 g) was dissolved in 50 mL of hydrazine hydrate and refluxed for 1.0 hr. The reaction mixtures were then poured in ice water. The precipitate was then filtered, washed with water and dried in a vacuum oven to afford the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06855730B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-85f8d0a13c1741908216e141c66ffd9d |
| Quellennotiz | uspto-grants-2005_02 |