HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Fluoro-2-iodobenzoic acid → 4-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Fluoro-2-iodobenzoic acid | HCID 12520164 | — |
| Edukt | 5-Fluoro-2-iodobenzoic acid | HCID 13158583 | — |
| Edukt | 5-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086948 | — |
| Produkt | 4-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086886 | — |
Reaktionsschritte
The title compound was prepared in a manner analogous to Intermediate 1, substituting for 4-fluoro-2-iodo-benzoic acid for 5-fluoro-2-iodo-benzoic acid in Step A. 1H NMR (400 MHz, CD3OD): 7.93 (s, 2H), 7.88 (dd, J=8.7, 5.9 Hz, 1H), 7.56 (dd, J=9.2, 2.5 Hz, 1H), 7.38-7.30 (m, 1H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08653263B2 |
| Quelldatensatz | uspto-grants-2014_02 |
| ORD ID | ord-78d3057ed8b442fca83afa37a40eb5b1 |
| Quellennotiz | uspto-grants-2014_02 |