HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Iodo-6-methylbenzoic acid → 2-methyl-6-(2H-1,2,3-triazol-2-yl)benzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Iodo-6-methylbenzoic acid | HCID 9856531 | — |
| Edukt | 5-Fluoro-2-iodobenzoic acid | HCID 13158583 | — |
| Edukt | 5-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086948 | — |
| Produkt | 2-methyl-6-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086973 | — |
Reaktionsschritte
The title compound was prepared in a manner analogous to Intermediate 1, substituting for 2-iodo-6-methyl benzoic acid for 5-fluoro-2-iodo-benzoic acid in Step A. 1H NMR (400 MHz, CD3OD): 7.89 (s, 2H), 7.72 (d, J=8.1 Hz, 1H), 7.48 (t, J=7.9 Hz, 1H), 7.36 (d, J=7.7 Hz, 1H), 2.46 (s, 3H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08653263B2 |
| Quelldatensatz | uspto-grants-2014_02 |
| ORD ID | ord-947af9e3a1c74d8699b60108e885e149 |
| Quellennotiz | uspto-grants-2014_02 |