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HRID 24613Erstellt: 23. Oktober 2026

3,3-Diphenylpropylamine → Benzyl 4-(3-chlorophenyl)-3-(3,3-diphenylpropylcarbamoyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

https://huagongshe.com/de/reaction/24613

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3,3-DiphenylpropylamineHCID 79698—
Edukt5-benzyl 1-(4-nitrophenyl) 6-(3-chlorophenyl)-2-methoxy-4-methyl-6H-pyrimidine-1,5-dicarboxylateHCID 69745932—
LösungsmittelAcetonitrileHCID 6342—
ProduktBenzyl 4-(3-chlorophenyl)-3-(3,3-diphenylpropylcarbamoyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylateHCID 15546109—

Reaktionsbedingungen

Temperatur60 °C

Reaktionsschritte

10 ml of acetonitrile was added to a mixture of 200 mg (0.373 mmol) of 5-benzyl 1-(4-nitrophenyl) 6-(3-chlorophenyl)-2-methoxy-4-methyl-6H-pyrimidine-1,5-dicarboxylate and 78.9 mg (0.373 mmol) of 3,3-diphenylpropylamine, and they were stirred at 60° C. for 30 minutes. The solvent was evaporated under reduced pressure to obtain the title compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06855716B2
Quelldatensatzuspto-grants-2005_02
ORD IDord-74147c16a95240d69ee024fbc23bdbd2
Quellennotizuspto-grants-2005_02