HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → 6-Hydroxyindole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | 3-Amino-p-cresol | HCID 17820 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Produkt | 6-Hydroxyindole | HCID 524508 | 38% |
Reaktionsschritte
The semicarbazone obtained above was reduced catalytically using 10% palladium on carbon in ethanol to yield a mixture of 6-hydroxyindole 38% yield, mp 124°-6° C., and 3-amino-4-methylphenol which were separated by column chromatography.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04704390 |
| Quelldatensatz | uspto-grants-1987_11 |
| ORD ID | ord-7cd80c3b6edb4a3a9f9b461fd0442c69 |
| Quellennotiz | uspto-grants-1987_11 |