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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 246898Erstellt: 25. Oktober 2026

Chlorine → 1-Chloro-4-(trifluoromethoxy)benzene

https://huagongshe.com/reaction/246898

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktChlorineHCID 24526—
Edukt1-Nitro-4-(trifluoromethoxy)benzeneHCID 522405—
Produkt1-Chloro-4-(trifluoromethoxy)benzeneHCID 277727383%

Reaktionsschritte

Chlorine and p-nitrotrifluoromethoxybenzene (10.7 parts) were fed simultaneously at a molar ratio of 3:1, Cl2 : organic reactant, into a vapor phase reactor maintained at 300° to 320° C. over a 30 minute period to yield 8.2 parts of p-chlorotrifluoromethoxybenzene (83% yield). The structure of the product was confirmed by gas chromatographic-mass spectrum and F19 nuclear magnetic resonance analysis.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04704483
Quelldatensatzuspto-grants-1987_11
ORD IDord-4cbebf0936474408b6dc36d8d22c9472
Quellennotizuspto-grants-1987_11