HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chlorine → 1-Chloro-4-(trifluoromethoxy)benzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chlorine | HCID 24526 | — |
| Edukt | 1-Nitro-4-(trifluoromethoxy)benzene | HCID 522405 | — |
| Produkt | 1-Chloro-4-(trifluoromethoxy)benzene | HCID 2777273 | 83% |
Reaktionsschritte
Chlorine and p-nitrotrifluoromethoxybenzene (10.7 parts) were fed simultaneously at a molar ratio of 3:1, Cl2 : organic reactant, into a vapor phase reactor maintained at 300° to 320° C. over a 30 minute period to yield 8.2 parts of p-chlorotrifluoromethoxybenzene (83% yield). The structure of the product was confirmed by gas chromatographic-mass spectrum and F19 nuclear magnetic resonance analysis.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04704483 |
| Quelldatensatz | uspto-grants-1987_11 |
| ORD ID | ord-4cbebf0936474408b6dc36d8d22c9472 |
| Quellennotiz | uspto-grants-1987_11 |